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Radical reaction of isocyanide with thiol

โœ Scribed by Saegusa, Takeo.; Kobayashi, Shiro.; Ito, Yoshihiko.

Book ID
126172910
Publisher
American Chemical Society
Year
1970
Tongue
English
Weight
510 KB
Volume
35
Category
Article
ISSN
0022-3263

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Alkenyl and alkynyl isocyanides were synthesised and then reacted, using microwave flash-heating technology, with thiophenol, 2-mercaptoethanol and ethanethiol, in the presence of a radical initiator, to give highly functionalised pyrrolines and pyroglutamates. Direct comparison with results obtaine