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ChemInform Abstract: Thiol-Mediated Free Radical Cyclization of Alkenyl and Alkynyl Isocyanides.

โœ Scribed by M. D. BACHI; A. BALANOV; N. BAR-NER

Book ID
112022693
Publisher
John Wiley and Sons
Year
2010
Weight
31 KB
Volume
26
Category
Article
ISSN
0931-7597

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Alkenyl and alkynyl isocyanides were synthesised and then reacted, using microwave flash-heating technology, with thiophenol, 2-mercaptoethanol and ethanethiol, in the presence of a radical initiator, to give highly functionalised pyrrolines and pyroglutamates. Direct comparison with results obtaine