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Microwave-Assisted Free-Radical Cyclization of Alkenyl and Alkynyl Isocyanides with Thiols.

โœ Scribed by Massimiliano Lamberto; David F. Corbett; Jeremy D. Kilburn

Publisher
John Wiley and Sons
Year
2003
Weight
262 KB
Volume
34
Category
Article
ISSN
0931-7597

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โœฆ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

๐Ÿ“œ SIMILAR VOLUMES

Microwave assisted free radical cyclisat
Microwave assisted free radical cyclisation of alkenyl and alkynyl isocyanides with thiols
โœ Massimiliano Lamberto; David F. Corbett; Jeremy D. Kilburn ๐Ÿ“‚ Article ๐Ÿ“… 2003 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 164 KB

Alkenyl and alkynyl isocyanides were synthesised and then reacted, using microwave flash-heating technology, with thiophenol, 2-mercaptoethanol and ethanethiol, in the presence of a radical initiator, to give highly functionalised pyrrolines and pyroglutamates. Direct comparison with results obtaine