A method for separation of amino acid methyl or phenyl thiohydantoins by GLC on a short glass capillary column is described. Calculations of required parameters of the capillary column are presented. By the described methods, nineteen of twenty silylated methylthiohydantoins were separated in one ru
✦ LIBER ✦
Quantitative gas chromatographic analysis of amino acids on a short glass capillary column
✍ Scribed by Jörgen Jönsson; Julius Eyem; John Sjöquist
- Book ID
- 118308724
- Publisher
- Elsevier Science
- Year
- 1973
- Tongue
- English
- Weight
- 801 KB
- Volume
- 51
- Category
- Article
- ISSN
- 0003-2697
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Sugars were separated gas chromatographically on short apolar glass capillary columns by using cold, on-column injection (OCI) techniques. After silylation, oligomers up to the hexasaccharides could be efficiently separated in reasonable retention times. Response factors of silylated sugars were det