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Gas chromatographic separation of sugars by on-column injection on glass capillary columns

✍ Scribed by Traitler, H. ;Del Vedovo, S. ;Schweizer, T. F.

Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
313 KB
Volume
7
Category
Article
ISSN
0935-6304

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✦ Synopsis

Sugars were separated gas chromatographically on short apolar glass capillary columns by using cold, on-column injection (OCI) techniques. After silylation, oligomers up to the hexasaccharides could be efficiently separated in reasonable retention times. Response factors of silylated sugars were determined as a function of varying sample amounts anld concentrations. The optimum injection amount was found to be 1 pl in heptane as solvent.

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