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Quantification of urinary 3α,21-dihydroxy-5β-pregnan-20-one and 5-pregnene-3β, 20α-diol by mass fragmentography

✍ Scribed by Louise P. Romanoff; Harry J. Brodie


Book ID
116000481
Publisher
Elsevier Science
Year
1976
Tongue
English
Weight
704 KB
Volume
7
Category
Article
ISSN
0022-4731

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Synthesis of 5α-pregnane-3β,20α-diol and
✍ T. A. Baillie; J. E. Herz; J. Sjövall 📂 Article 📅 1974 🏛 John Wiley and Sons 🌐 French ⚖ 241 KB 👁 1 views

## Abstract A convenient synthesis of 5α‐[20β‐^2^H]pregnane‐3α,20α‐diol and 5α‐[20β‐^2^H]pregnane‐3β,20α‐diol from 3β‐hydroxy‐5α‐pregn‐16‐en‐20‐one is described. The reaction products are characterized by combined gas chromatography‐mass spectrometry.