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Propellanes V. [3.3.1] Propellane

✍ Scribed by Philip Warner; Richard LaRose; Thomas Schleis

Publisher
Elsevier Science
Year
1974
Tongue
French
Weight
181 KB
Volume
15
Category
Article
ISSN
0040-4039

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## Abstract 3,7,10‐Tribenzyl‐3,7,10‐triaza[3.3.3]propellane (**4a**), 3,7‐dibenzyl‐10‐phenyl‐3,7,10‐triaza[3.3.3]propellane (**4c**), 3,7‐dibenzyl‐10‐(__p__‐tolyl)‐3,7,10‐triaza[3.3.3]propellane (**4b**), and 3‐oxa‐7,10‐diaza[3.3.3]propellane (**6**) have been prepared.

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## Abstract Oxidation of the title compound with __m__‐chloroperbenzoic acid affords a keto‐lactone, two bis‐lactones and a bis‐spirolactone, in varying amounts depending upon the reaction conditions. The structures were established by means of X‐ray diffraction, ^1^H‐ and ^13^C‐NMR spectroscopy.