## Abstract Procedures for the preparation of N‐feruloylglycine (II), ‐DL‐alanine (XX), ‐DL‐valine (XXII) and ‐L‐leucine (XXIV) by classical methods are proposed and compared. The spectral characteristics and Rf‐values of the substances are included. The compounds were synthesized because N‐feruloy
Production of peptides and arylthioesters of N-acylamino acids using arylsulfenyl chlorides
✍ Scribed by Yu. V. Mitin; G. P. Vlasov; G. I. Shelykh
- Book ID
- 112434040
- Publisher
- Springer
- Year
- 1967
- Tongue
- English
- Weight
- 59 KB
- Volume
- 16
- Category
- Article
- ISSN
- 1573-9171
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## Abstract As a result of difficulties with the synthesis of pure O‐(m)ethoxycarbonylferulyl chloride, N‐ferulylglycyl‐L‐phenylalanine (XVI) was previously prepared by a mixed anhydride method. However, due to the fact that analogous N‐acyl‐dipeptides were easily obtained by the acid chloride meth
## Abstract N‐(Feruloyl‐2‐^14^C)‐glycine‐2‐^3^H (IX) was obtained with an acceptable yield (43%) starting from O‐methoxycarbonyl‐ferulic acid‐2‐^14^C (IV) and glycine‐2‐^3^H ethyl ester (VI). The latter two compounds were first condensed into N‐(O‐methoxycarbonyl‐feruloyl‐2‐^14^C)‐glycine ‐2‐^3^H e