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Preparation of tritium labelled synthanecine a and its bis-N-ethylcarbamate

✍ Scribed by A. Robin Mattocks

Publisher
John Wiley and Sons
Year
1982
Tongue
French
Weight
188 KB
Volume
19
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A procedure is described for incorporating tritium into the 3‐CH~2~ side chain of synthanecine A, and preparing the carbamate, 2,3‐bis‐N‐ethylcarbamoyloxymethyl‐l‐methyl‐3‐pyrroline, a hepatotoxic pyrrolizidine alkaloid analogue. The pyrrolizidine amino alcohol, retronecine, can be tritium labelled in a similar way.

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