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Preparation of phenamine-C14of high specific activity

✍ Scribed by N. A. Kogan; B. Z. Askinazi; M. I. Vlasova; N. Ya. Kozarinskaya

Book ID
112396878
Publisher
Springer
Year
1976
Tongue
English
Weight
147 KB
Volume
10
Category
Article
ISSN
0091-150X

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## Abstract N,N‐[Methyl‐^14^C]‐Dimethylhydrazine hydrochloride () having a specific activity of 115 mCi/mmol, was synthesized in two steps. Dimethylation of acetophenone hydrazone with ^14^C‐methyl iodide (specific activity = 58 mCi/mmol) in the presence of potassium in liquid ammonia followed by a