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Preparation of 6-deoxy-D-[U-14C]glucose

✍ Scribed by V. Siglerová; K. Vereš


Publisher
John Wiley and Sons
Year
1989
Tongue
French
Weight
208 KB
Volume
27
Category
Article
ISSN
0022-2135

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Labeled 2-deoxy-D-glucose analogs. 18F-l
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## Abstract A convenient method for the synthesis of ^18^F‐2‐deoxy‐2‐fluoro‐D‐glucose (4) and ^18^F‐2‐deoxy‐2‐fluoro‐D‐mannose (8) by the direct fluorination of 3,4,6‐tri‐0‐acetyl‐D‐glucal with ^18^F‐F~2~ is described. ^14^C‐2‐deoxy‐2‐fluoro‐D‐glucose has been synthesized from ^14^C‐3,4,6‐tri‐0‐ace

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## Abstract [U‐^14^C]Isosorbide and [U‐^14^C]dimethyl isosorbide with a specific activity of 462 MBq/mmol was prepared from D‐[U‐^14^C]glucose, in an overall yield of 79%, under microwave heating conditions. Copyright © 2006 John Wiley & Sons, Ltd.