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Preparation and Antibacterial Activity of 3-Methyl-1-p-substituted Phenylpyrazole-5-thiol

✍ Scribed by Yoshinobu Tagawa; Shin'ichi Minami; Toshio Yoshida; Keitaro Tanaka; Shuji Sato; Yoshinobu Goto; Kenji Yamagata

Publisher: John Wiley and Sons
Year: 2002
Tongue: English
Weight: 79 KB
Volume: 335
Category: Article
ISSN: 0365-6233
DOI: 10.1002/1521-4184(200203)335:2/3<99::aid-ardp99>3.0.co;2-2

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composition, and IR spectrumi3] with the product prepared from SOClz and HzS,. This new, more productive synthetic route requires much less time and experimental effort than the former preparation. ## Procedtwe: Sg (3.76g, 14.7mmol)isdissolved in CHzC12 (800ml) by refluxing. The homogeneous soluti