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Poly­[(1,10-phenanthroline-κ2N,N′)­lead(II) μ4-(4-sulfonatobenzoato-κ4O,O′:O′′,O′′′ hydrate]

✍ Scribed by Zhang, Li-Ping ;Zhu, Long-Guan ;Xiao, Hong-Ping

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
232 KB
Volume
61
Category
Article
ISSN
1600-5368

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In the title dimeric complex, [Cu~2~(C~2~O~4~)Cl~2~(C~12~H~8~N~2~)~2~], which lies on a crystallographic inversion center, the Cu^II^ ion is in a distorted trigonal–bipyramidal coordination geometry formed by two N atoms from a phen ligand, two O atoms from a bridging oxalate ligand and one Cl atom.

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Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.006 A Ê R factor = 0.040 wR factor = 0.062 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Poly­[[[(1,10-phenanthroline-κ2N,N′)­cob
Poly­[[[(1,10-phenanthroline-κ2N,N′)­cobalt(II)]-μ3-5-hydroxy­isophthalato-κ4O,O′:O′′:O′′′] monohydrate]
✍ Cao, Xin-Yi ;Zhang, Jian ;Kang, Yao ;Cheng, Jian-Kai ;Li, Zhao-Ji ;Wang, Xiao-Qi 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 334 KB

The title compound, {[Co(C 8 H 4 O 5 )(C 12 H 8 N 2 )]ÁH 2 O} n , is isostructural with its manganese analog [Skakle, Foreman & Plater (2001). Acta Cryst. E57, m373±m375]. The asymmetric unit consists of one Co atom, one 1,10-phenanthroline ligand bound in a bidentate manner, one hydroxyisophthalate