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(Piperidine-κN)[N-(salicyl­idene)­phenyl­alaninato-κ3O,N,O′]copper(II)

✍ Scribed by Butcher, Ray J. ;Mockler, Garry M. ;McKern, Owen

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
384 KB
Volume
59
Category
Article
ISSN
1600-5368

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The tridentate Schiff base ligand derived from the condensation of salicylaldehyde and dl-tyrosine, in the presence of pyridine, forms a square-pyramidal ®ve-coordinate Cu complex, [Cu(C 16 H 13 NO 4 )(C 5 H 5 N)(H 2 O)], with a water molecule occupying the apical site.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.045 wR factor = 0.105 Data-to-parameter ratio = 11.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the crystal structure of the title compound, [Cu(C 11 H 9 -NO 5 )(H 2 O) 2 ]Á2H 2 O, in which N-(3-carboxy-2-hydroxybenzylidene)alaninate (H 3 ALS) is the Schiff base synthesized from l-alanine with 3-carboxysalicylaldehyde, the copper(II) ion is pentacoordinated in a square-pyramidal geometry, w