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Palladium-Catalyzed ortho -Selective CH Borylation of 2-Phenylpyridine and Its Derivatives at Room Temperature

✍ Scribed by Kuninobu, Yoichiro; Iwanaga, Takashi; Omura, Tetsuya; Takai, Kazuhiko

Book ID
120169816
Publisher
John Wiley and Sons
Year
2013
Tongue
English
Weight
368 KB
Volume
52
Category
Article
ISSN
0044-8249

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## Abstract **Pd and CO—ureally got me!** The title reaction proceeds efficiently at 18 °C under CO (1 atm) with 5 % [Pd(OTs)~2~(MeCN)~2~] as precatalyst. Depending on the solvents used, either anthranilates or cyclic imides can be obtained in high yields (see picture, BQ=benzoquinone, Ts=4‐toluene