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(p-Toluene­sulfonato)tris­(triphenyl­arsine)silver(I)

✍ Scribed by Meijboom, Reinout ;Janse van Rensburg, J. Marthinus ;Senekal, Nadine D. ;Venter, Jacobus S.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
161 KB
Volume
62
Category
Article
ISSN
1600-5368

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The title compound, [Ag(AsC 18 H 15 ) 4 ]PF 6 , crystallizes with the cation on a threefold rotation axis and the anions on positions with site symmetry 3. The Ag atom is surrounded by four arsine ligands forming a distorted tetrahedral configuration. The Ag-As distances are 2.6381 (6) and 2.6499 (9

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In the title compound, [AgI(C 21 H 21 P) 3 ], important bond distances are: Ag-P = 2.5346 (9), 2.5562 (9) and 2.5617 (9) A ˚, and Ag-I = 2.8683 (5) A ˚. The Ag I atom is in a distorted tetrahedral environment and all bond angles are close to the ideal values.

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In the title compound, [Ag(C 2 H 3 O 2 )(C 18 H 15 As) 3 ]ÁC 2 H 3 NÁ-H 2 O, the Ag atom is coordinated by three arsine ligands and one O atom, forming a distorted tetrahedral configuration. The Ag-As bond distances are 2.5921 (6), 2.6190 (8) and 2.6373 (9) A ˚, and the Ag-O bond distance is 2.3269

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The title compound, [Ag 2 I 2 (C 5 H 5 N) 2 (C 21 H 21 P) 2 ], has C i molecular symmetry. Each Ag atom is surrounded by a phosphine ligand, a pyridine ligand and two iodide anions in a distorted tetrahedral coordination. The AgÁ Á ÁAg separation in the binuclear species is 3.1130 (18) A ˚. The Ag-P

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Single-crystal X-ray study T = 295 K Mean (C-C) = 0.007 A R factor = 0.038 wR factor = 0.102 Data-to-parameter ratio = 21.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.