𝔖 Bobbio Scriptorium
✦   LIBER   ✦

On-column injection on capillary columns with conventional injectors

✍ Scribed by Rinderknecht, F. ;Wenger, B.

Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
146 KB
Volume
4
Category
Article
ISSN
0935-6304

No coin nor oath required. For personal study only.

✦ Synopsis

negative chemical ionization spectra of TCDDs [12]. Conversely, no mechanism similarto the formation of a dichlorobenzoquinone anion of TCDD [lo] was detected for the three TCDF isomers. Also, no molecular anion was observed for any of the TCDF isomers investigated.

πŸ“œ SIMILAR VOLUMES

Direct injection of large sample volumes
Direct injection of large sample volumes into capillary columns with packed column injector
✍ Watanabe, Chuichi ;Hashimoto, Keiji πŸ“‚ Article πŸ“… 1990 πŸ› John Wiley and Sons 🌐 English βš– 381 KB

## Abstract A direct injection method for large volume samples which avoids severe tailing of the solvent peak has been developed using a packed column injector (up to 100 ΞΌl) leading into an ordinary capillary column (0.3 mm i.d.). Modifications are made to the cooler zones of the inlet port and o

Underivatized steroids on persilanized c
Underivatized steroids on persilanized capillary columns with non-vaporizing on-column injection
✍ Kovarich, E. ;Munari, F. πŸ“‚ Article πŸ“… 1982 πŸ› John Wiley and Sons 🌐 English βš– 381 KB

## Abstract Recent developments in the preparation of capillary columns by persilanization of the glass surfaces have resulted in highly inactive, heat‐stable columns. With this type of column certain steroid hormone classes can be analyzed without derivatization; these include the 17‐keto steroids

Large Volume Injection in Fast Gas Chrom
Large Volume Injection in Fast Gas Chromatography with On-Column Injector
✍ KorytΓ‘r, Peter ;MatisovΓ‘, Eva ;LefflerovΓ‘, Henrieta ;SlobodnΓ­k, Jaroslav πŸ“‚ Article πŸ“… 2000 πŸ› John Wiley and Sons 🌐 English βš– 87 KB

In this work a fast gas chromatography set-up with on-column injection was optimized and evaluated with a model mixture of C 8 -C 28 nalkanes. Usual injection volumes when using narrow-bore (e. g., 0.1 mm i.d.) analytical columns are ca. 0.1 lL. The presented configuration allows introduction of 10