Notes - Synthesis of DL-Norleucine-2-C 14
โ Scribed by Kaneko, Jiro; Black, Arthur; Kleiber, Max
- Book ID
- 126160242
- Publisher
- American Chemical Society
- Year
- 1958
- Tongue
- English
- Weight
- 281 KB
- Volume
- 23
- Category
- Article
- ISSN
- 0022-3263
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๐ SIMILAR VOLUMES
A new method of synthesis of DL-[ 7-14C]indospicine and DL-2-amino-[ 7-1 4C]pimelic acid and their nonradioactive equivalents is reported. The combined radiochemical yield of both compounds, starting from potassium 1 14C]cyanide was 15.3%. Indospicine was isolated as the flavianate.
D L -t y r o ~i n e -4 -~~C has been synthesized with an overall yield 29.3 based on phenol-1-14C as the starting material. Anisole-l-14C was prepared by methylation of phenol-1-14C with dimethyl sulfate. The radioactive anisole was then converted to p-anisaldehyde-4-14C by a modijied Gattermann rea