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N,N-Bis(2-pyridinio­methyl)­glycine diperchlorate

✍ Scribed by Nielsen, Anne ;Bond, Andrew D. ;McKenzie, Christine J.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
173 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the crystal structure of the title compound, C 14 H 17 -N 3 O 2 2+ Á2ClO 4 À , at 180 K, OÐHÁ Á ÁO hydrogen-bonded dimers are formed across inversion centres.

📜 SIMILAR VOLUMES

N-Methyl-N-(2-pyridinio­methyl)-2-[N-(2-
N-Methyl-N-(2-pyridinio­methyl)-2-[N-(2-pyridinio­methyl)­methyl­amino]-N-(2-pyridyl­methyl)­ethanaminium tris(perchlorate)
✍ Rompel, Annette ;Bond, Andrew D. ;McKenzie, Christine J. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 234 KB

Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.004 A Ê R factor = 0.056 wR factor = 0.154 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N,N,N′,N′-Tetrakis(2-pyridinio­methyl)­e
N,N,N′,N′-Tetrakis(2-pyridinio­methyl)­ethyl­enedi­amine tetraperchlorate
✍ Gunatilleke, Shamila S. ;Norman, Richard E. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 209 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.004 A Ê R factor = 0.061 wR factor = 0.111 Data-to-parameter ratio = 11.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N,N′-Bis­(amino­propyl)-1,4-benzyl­idene
N,N′-Bis­(amino­propyl)-1,4-benzyl­idenedi­ammonium diperchlorate
✍ Yang, Shi-Ping ;Chen, Hong-Mei ;Znang, Fan ;Yu, Xi-Bin ;Weng, Lin-Hong 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 340 KB

The structure determination of the title compound, [C 14 H 24 N 4 ](ClO 4 ) 2 , indicates that intermolecular hydrogen bonds between the N atom of the aminopropyl group and an O atom of the perchlorate result in a two-dimensional layer structure. The cation has crystallographic inversion symmetry.

μ-Oxo-bis{chloro­[N,N′-di­methyl-N,N′-bi
μ-Oxo-bis{chloro­[N,N′-di­methyl-N,N′-bis(2-pyridyl­methyl)­ethane-1,2-di­amine]iron(III)} diperchlorate 0.751-hydrate
✍ Egdal, Rune Kirk ;Hazell, Alan ;McKenzie, Christine J. 📂 Article 📅 2001 🏛 International Union of Crystallography 🌐 English ⚖ 345 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.032 wR factor = 0.034 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.