In the crystal structure of the title compound, C 14 H 17 -N 3 O 2 2+ Á2ClO 4 À , at 180 K, OÐHÁ Á ÁO hydrogen-bonded dimers are formed across inversion centres.
N-Methyl-N-(2-pyridiniomethyl)-2-[N-(2-pyridiniomethyl)methylamino]-N-(2-pyridylmethyl)ethanaminium tris(perchlorate)
✍ Scribed by Rompel, Annette ;Bond, Andrew D. ;McKenzie, Christine J.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 234 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.004 A Ê R factor = 0.056 wR factor = 0.154 Data-to-parameter ratio = 14.9
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.004 A Ê R factor = 0.061 wR factor = 0.111 Data-to-parameter ratio = 11.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 113 K Mean '(C±C) = 0.005 A Ê R factor = 0.056 wR factor = 0.163 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title vanadium complex, [VClO(C 16 H 22 N 4 )]ClO 4 , of the tetradentate ligand N,N H -dimethyl-N,N H -bis(2-pyridylmethyl)ethane-1,2-diamine was obtained from air oxidation of a mixture of the ligand and VCl 3 in wet methanol.
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.088 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.