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N-[4-Cyano-3-(trifluoro­methyl)phenyl]-3-(4-fluoro­phenyl­sulfanyl)-2-hydroxy-2-methyl­propionamide chloro­form solvate

✍ Scribed by Tang, Gu-Ping ;Gu, Jian-Ming

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
250 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 18 H 14 F 4 N 2 O 2 SÁCHCl 3 , forms a onedimensional hydrogen-bonded chain via a single O-HÁ Á ÁN interaction; the chain runs approximately along the [110] axis. The two benzene rings are almost parallel to one another, forming a dihedral angle of 8.43 (8) .

📜 SIMILAR VOLUMES

N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]
N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]-3-(4-fluoro­phenyl­sulfan­yl)-2-hydr­oxy-2-methyl­propionamide
✍ Hu, Xiu-Rong ;Wang, Li-Li ;Gu, Jian-Ming 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 201 KB

Single-crystal X-ray study T = 296 K Mean (C-C) = 0.004 A Disorder in main residue R factor = 0.065 wR factor = 0.175 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]
N-[4-Cyano-3-(trifluoro­meth­yl)phen­yl]-3-(4-fluoro­phenyl­sulfon­yl)-2-hydr­oxy-2-methyl­propionamide
✍ Hu, Xiu-Rong ;Gu, Jian-Ming 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 254 KB

The structure of the title compound, C 18 H 14 F 4 N 2 O 2 S, consists of molecules that pack in a linear hydrogen-bonded chain along the c axis. This hydrogen-bonding arrangement involves the hydroxy group and one of the sulfonyl O atoms.

N-(3-Chloro-4-methyl­phenyl)-N′-hydroxy-
N-(3-Chloro-4-methyl­phenyl)-N′-hydroxy-2-oxo-2-phenyl­acet­amidine
✍ Hökelek, Tuncer ;Büyükgüngör, Orhan ;Taş, Murat ;Batı, Hümeyra 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 471 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.041 wR factor = 0.100 Data-to-parameter ratio = 19.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

3-[(2-Chloro­phenyl)­sulfonyl­amino]-2-c
3-[(2-Chloro­phenyl)­sulfonyl­amino]-2-cyano-N-(3,5-di­methoxy­phenyl)-3-methyl­sulfanyl-2-propen­amide
✍ Kennard, Colin H. L. ;McFadden, Helen G. ;Byriel, Karl A. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 178 KB

In the title compound, C 19 H 18 ClN 3 O 5 S 2 , which is a representative of a class of inactive acetolactate synthase inhibitors, the dihedral angle between the two aromatic groups is 85.9 (1) .