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3-[(2-Chloro­phenyl)­sulfonyl­amino]-2-cyano-N-(3,5-di­methoxy­phenyl)-3-methyl­sulfanyl-2-propen­amide

✍ Scribed by Kennard, Colin H. L. ;McFadden, Helen G. ;Byriel, Karl A.

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
178 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 19 H 18 ClN 3 O 5 S 2 , which is a representative of a class of inactive acetolactate synthase inhibitors, the dihedral angle between the two aromatic groups is 85.9 (1) .

📜 SIMILAR VOLUMES

Ethyl 3-{[(2-chloro­phenyl)­sulfonyl]­im
Ethyl 3-{[(2-chloro­phenyl)­sulfonyl]­imino}-2-{[(3,5-di­methoxy­phenyl)­amino]­carbonyl}-3-(methyl­sulfanyl)­propanoate
✍ Kennard, Colin H. L. ;McFadden, Helen G. ;Byriel, Karl A. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 314 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.010 A Ê Disorder in main residue R factor = 0.043 wR factor = 0.152 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N-[4-Cyano-3-(trifluoro­methyl)phenyl]-3
N-[4-Cyano-3-(trifluoro­methyl)phenyl]-3-(4-fluoro­phenyl­sulfanyl)-2-hydroxy-2-methyl­propionamide chloro­form solvate
✍ Tang, Gu-Ping ;Gu, Jian-Ming 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 250 KB

The title compound, C 18 H 14 F 4 N 2 O 2 SÁCHCl 3 , forms a onedimensional hydrogen-bonded chain via a single O-HÁ Á ÁN interaction; the chain runs approximately along the [110] axis. The two benzene rings are almost parallel to one another, forming a dihedral angle of 8.43 (8) .

N-[2-(3,4-Di­methoxy­phenyl)­ethyl]-3-ph
N-[2-(3,4-Di­methoxy­phenyl)­ethyl]-3-phenyl­acryl­amide
✍ Ohba, Shigeru ;Ito, Yoshikatsu 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 339 KB

Single-crystal X-ray study T = 250 K Mean '(C±C) = 0.004 A Ê R factor = 0.056 wR factor = 0.156 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-(3,5-Di­methoxy­phenyl)-2-{2-[(3,5-dim
1-(3,5-Di­methoxy­phenyl)-2-{2-[(3,5-dimethoxy­phenyl)­hydroxy­methyl]-4-methoxy­phenyl}ethanol
✍ Yin, Qiang ;Zhang, Wen-Qin 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 416 KB

The title compound, C 26 H 30 O 7 , was obtained by the Grignard reaction of one molecule of 4-methoxybenzylmagnesium chloride with two molecules of 3,5-dimethoxybenzaldehyde. The two new chiral centers have the same absolute con®guration R (S), and the two hydroxyl groups, surrounded by the three b