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N-[2-(3,4-Di­methoxy­phenyl)­ethyl]-3-phenyl­acryl­amide

✍ Scribed by Ohba, Shigeru ;Ito, Yoshikatsu


Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
339 KB
Volume
58
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 250 K Mean '(C±C) = 0.004 A Ê R factor = 0.056 wR factor = 0.156 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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The title compound, C 26 H 30 O 7 , was obtained by the Grignard reaction of one molecule of 4-methoxybenzylmagnesium chloride with two molecules of 3,5-dimethoxybenzaldehyde. The two new chiral centers have the same absolute con®guration R (S), and the two hydroxyl groups, surrounded by the three b