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N-(4-Chlorophenyl)-N-(4,5-dihydro-1H-imidazol-2-yl)amine formamide solvate

✍ Scribed by Yıldırım, Sema Öztürk ;Akkurt, Mehmet ;Servi, Süleyman ;Şekerci, Memet ;Heinemann, Frank W.

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
257 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 9 H 10 ClN 3 ÁHC(O)NH 2 , the benzene and imidazole rings make a dihedral angle of 43.3 (1) . In the crystal structure, molecules are linked through weak intermolecular N-HÁ Á ÁO, N-HÁ Á ÁN and C-HÁ Á ÁN hydrogen bonds, forming a three-dimensional framework.

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2,6-Diamino-4-(4-methoxy­phen­yl)-1,4-di
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The title compound, C 14 H 11 N 5 OÁC 3 H 7 NO, was synthesized by the reaction of 4-methoxybenzaldehyde with malononitrile and ammonium acetate under microwave irradiation. The dihedral angle between the pyridine and benzene planes is 56.07 (8) .

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✍ He, Hong-Shan 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 125 KB

In the title complex, [Ni(C 9 H 9 N 2 O) 2 ], the Ni 2+ ion is coordinated by two 2-(4,5-dihydro-1H-imidazol-2-yl)phenolate ligands. Each ligand provides one O atom and one N atom to the Ni coordination, giving a total coordination number of 4. The centrosymmetric complex adopts a square-planar geom

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✍ Shi, Jun 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 180 KB

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.006 A Disorder in solvent or counterion R factor = 0.046 wR factor = 0.133 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4-(4-Chloro­phen­yl)-N-phenyl-5-(1H-1,2,
4-(4-Chloro­phen­yl)-N-phenyl-5-(1H-1,2,4-triazol-1-yl)thia­zol-2-amine
✍ Shao, Ling ;Zhou, Xin ;Fang, Jian-Xin 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 193 KB

The title compound, C 17 H 12 ClN 5 S, has been synthesized as a potent anticancer agent. The dihedral angle between the thiazole and triazole rings is 85.9 (2) . There are intermolecular N-HÁ Á ÁN and C-HÁ Á ÁCl interactions in the crystal structure.