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N′-[1-(4-Chlorophenyl)ethylidene]acetohydrazine

✍ Scribed by Guo, Huan-Mei

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
440 KB
Volume
63
Category
Article
ISSN
1600-5368

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The title compound, C~9~H~10~CIN~3~S, was prepared by the reaction of thiosemicarbazide with 1-(2-chlorophenyl)ethanone at room temperature. The packing is stabilized by hydrogen bonds. In the crystal structure, molecules are linked into two-dimensional layers by intermolecular N—H...S hydrogen-bond

N′-[1-(2,4-Difluorophenyl)ethylidene]-4-
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✍ Shang, Zhen-Hua 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 703 KB

The title compound, C~15~H~14~F~2~N~2~O~2~S, was synthesized by the reaction of 1-(2,4-difluorophenyl)ethanone and 4-methylbenzenesulfonohydrazide in ethanol under reflux. The crystal structure is stabilized mainly through intermolecular N—H...O hydrogen bonds. The C=N—N group displays a __trans__ c