N-3,5-Dimethyl-[1-(4-nitrophenyl)ethylidene]aniline
✍ Scribed by Yang, Xiu-Ying ;Li, Yu-Feng ;Zheng, Jian ;Jian, Fang-Fang
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 134 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 9 H 10 N 4 O 2 S, was prepared by the reaction of thiosemicarbazide with 1-(3-nitrophenyl)ethanone at room temperature. The crystal packing is stabilized by van der Waals forces.
In the title compound, C 16 H 17 N 5 O 2 S, the configuration is trans about the formal C N bond. The molecular conformation is stabilized by an intramolecular N-HÁ Á ÁN hydrogen bond.
Single-crystal X-ray study T = 113 K Mean (C-C) = 0.002 A Disorder in solvent or counterion R factor = 0.044 wR factor = 0.120 Data-to-parameter ratio = 14.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.