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1-[1-(3-Nitro­phen­yl)ethyl­idene]thio­semicarbazide

✍ Scribed by Wang, Jian-Gang ;Jian, Fang-Fang ;Qin, Yong-Qi ;Wang, Yan

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
119 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 9 H 10 N 4 O 2 S, was prepared by the reaction of thiosemicarbazide with 1-(3-nitrophenyl)ethanone at room temperature. The crystal packing is stabilized by van der Waals forces.

📜 SIMILAR VOLUMES

1-[1-(2-Chloro­phen­yl)ethyl­idene]thio­
1-[1-(2-Chloro­phen­yl)ethyl­idene]thio­semicarbazide
✍ Wang, Jian-Gang ;Jian, Fang-Fang ;Ren, Xiao-Yan ;Kan, Shi-Hong 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 154 KB

The title compound, C~9~H~10~CIN~3~S, was prepared by the reaction of thiosemicarbazide with 1-(2-chlorophenyl)ethanone at room temperature. The packing is stabilized by hydrogen bonds. In the crystal structure, molecules are linked into two-dimensional layers by intermolecular N—H...S hydrogen-bond

4-Phen­yl-1-(1-phenyl­ethyl­idene)thio­s
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✍ Jian, Fangfang ;Li, Ying ;Xiao, Hailian 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 85 KB

View of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.

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✍ Fang, Wei ;Lin, Li-Rong ;Huang, Rong-Bin ;Zheng, Lan-Sun 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 144 KB

In the title compound, C 16 H 17 N 5 O 2 S, the configuration is trans about the formal C N bond. The molecular conformation is stabilized by an intramolecular N-HÁ Á ÁN hydrogen bond.