1-[1-(2-Chlorophenyl)ethylidene]thiosemicarbazide
✍ Scribed by Wang, Jian-Gang ;Jian, Fang-Fang ;Ren, Xiao-Yan ;Kan, Shi-Hong
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 154 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C~9~H~10~CIN~3~S, was prepared by the reaction of thiosemicarbazide with 1-(2-chlorophenyl)ethanone at room temperature. The packing is stabilized by hydrogen bonds. In the crystal structure, molecules are linked into two-dimensional layers by intermolecular N—H...S hydrogen-bonding interactions.
📜 SIMILAR VOLUMES
The title compound, C 9 H 10 N 4 O 2 S, was prepared by the reaction of thiosemicarbazide with 1-(3-nitrophenyl)ethanone at room temperature. The crystal packing is stabilized by van der Waals forces.
View of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.113 Data-to-parameter ratio = 19.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
View of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.