Benzyl N-[1-(thiophen-2-yl)ethylidene)]hydrazinecarbodithioate
✍ Scribed by Chan, Mun-Hoe Eddy ;Crouse, Karen A. ;Tarafder, M. T. H. ;Yamin, Bohari. M.
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 290 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.113 Data-to-parameter ratio = 19.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound, C~9~H~10~CIN~3~S, was prepared by the reaction of thiosemicarbazide with 1-(2-chlorophenyl)ethanone at room temperature. The packing is stabilized by hydrogen bonds. In the crystal structure, molecules are linked into two-dimensional layers by intermolecular N—H...S hydrogen-bond
The title compound, C 9 H 10 N 4 O 2 S, was prepared by the reaction of thiosemicarbazide with 1-(3-nitrophenyl)ethanone at room temperature. The crystal packing is stabilized by van der Waals forces.
View of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.
In the title compound, C 16 H 17 N 5 O 2 S, the configuration is trans about the formal C N bond. The molecular conformation is stabilized by an intramolecular N-HÁ Á ÁN hydrogen bond.