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4-Phen­yl-1-(1-phenyl­ethyl­idene)thio­semicarbazide

✍ Scribed by Jian, Fangfang ;Li, Ying ;Xiao, Hailian

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
85 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

View of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.

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The title compound, C 9 H 10 N 4 O 2 S, was prepared by the reaction of thiosemicarbazide with 1-(3-nitrophenyl)ethanone at room temperature. The crystal packing is stabilized by van der Waals forces.

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The title compound, C~9~H~10~CIN~3~S, was prepared by the reaction of thiosemicarbazide with 1-(2-chlorophenyl)ethanone at room temperature. The packing is stabilized by hydrogen bonds. In the crystal structure, molecules are linked into two-dimensional layers by intermolecular N—H...S hydrogen-bond

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View of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.

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In the title compound, C 16 H 17 N 5 O 2 S, the configuration is trans about the formal C N bond. The molecular conformation is stabilized by an intramolecular N-HÁ Á ÁN hydrogen bond.