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N-[1′-(2,4,6-Trimethylanilino)-1-ferrocenyl]-N-(2,4,6-trimethylphenyl)thiocarbamoyl chloride

✍ Scribed by Rupert, Benjamin L. ;Arnold, John

Publisher: International Union of Crystallography
Year: 2006
Tongue: English
Weight: 191 KB
Volume: 62
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536806028972

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✦ Synopsis

The title compound, [Fe(C 15 H 15 ClNS)(C 14 H 16 N)], crystallizes with the thiocarbamoyl chloride unit nearly coplanar with the cyclopentadienyl ring to which it is attached. There is a slight deviation from planarity which, along with the orientation of the amino substituent on the other cyclopentadienyl ring, is suggestive of an intramolecular hydrogen bond. The long donor-acceptor NÁ Á ÁS length of 3.702 (2) A ˚indicates that any interaction is weak.

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✦ Synopsis

N-[1′-(2,4,6-Trimethylanilino)-1-ferrocenyl]-N-(2,4,6-trimethylphenyl)thiocarbamoyl chloride