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O-[4-(2,2,4-Trimethyl­chroman-4-yl)phen­yl] N,N-dimethyl­thio­carbamate

✍ Scribed by Vries, Elise J. C. de ;Bredenkamp, Martin W. ;Jacobs, Tia ;Lloyd, Gareth O.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
259 KB
Volume
61
Category
Article
ISSN
1600-5368

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(S)-O-[4-(2,2,4-Trimethylchroman-4-yl)ph
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✍ Jacobs, Tia ;Bredenkamp, Martin W. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 722 KB

Crystallization of the (__S__)-enantiomer of the title compound, C~21~H~26~NO~2~S, from methanol gave an unsolvated crystal structure in which one-dimensional strands of molecules are formed through a series of C—H...O and C—H...S hydrogen bonds, and C—H...π interactions.

(E)-O-Ethyl N-(4-methyl­phen­yl)thio­car
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✍ Tadbuppa, Primjira P. ;Tiekink, Edward R. T. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 138 KB

The title compound, C 10 H 13 NOS, displays an E conformation about the central C-N bond and exists in the thione form. N-HÁ Á ÁS hydrogen-bonding interactions link centrosymmetrically related molecules into dimers. organic papers o1886 Tadbuppa and Tiekink C 10 H 13 NOS

(E)-O-Ethyl N-(4-nitro­phen­yl)thio­carb
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✍ Benson, Ronald E. ;Broker, Grant A. ;Daniels, Lee M. ;Tiekink, Edward R. T. ;War 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 250 KB

Single-crystal X-ray study T = 150 K Mean (C-C) = 0.003 A R factor = 0.052 wR factor = 0.162 Data-to-parameter ratio = 25.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.