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1-[3-Meth­yl-3-(2,4,6-trimethyl­phen­yl)cyclo­but­yl]-2-(thio­morpholin-4-yl)ethanone

✍ Scribed by Saraçoĝlu, Hanife ;Soylu, Serkan ;Çalıs˛kan, Nezihe ;Çukurovali, Alaaddin ;Yilmaz, Ibrahim ;Kazaz, Cavit

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
231 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The molecular structure of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme.

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✍ Wang, Hai-Bo ;Liu, Zhi-Qian ;Yan, Xiao-Chen 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 119 KB

The title compound, C 23 H 26 BrN 5 O 2 , was synthesized by the reaction of 4- [(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine and 3-(3-nitrophenyl)-5-chloromethyl-1,2,4-oxadiazole. There are intramolecular C-HÁ Á ÁN and intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds in the crystal struc

1-(3-Mesit­yl-3-methyl­cyclo­but­yl)-2-(
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In the title compound, C 21 H 31 NO, the cyclobutane ring is puckered, with a dihedral angle of 25.74 (6) . The mesityl and 2-N-piperidino-1-oxoethyl groups are in cis positions. The piperidine fragment adopts a chair conformation. Intermolecular C-HÁ Á ÁO interactions involving the piperidine CH gr