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4-{[3-(2-Chloro­phen­yl)-1,2,4-oxadiazol-5-yl]meth­yl}-1-[(2,6-dimethyl­phen­yl)amino­carbon­yl­meth­yl]piperazine

✍ Scribed by Wang, Hai-Bo ;Pu, Yue-Qing ;Chen, Jia-Hui ;Wang, Jin-Tang

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
174 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 23 H 26 ClN 5 O 2 , was synthesized by the reaction of 4- [(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine and 5-chloromethyl-3-(2-chlorophenyl)-1,2,4oxadiazole. In the structure, there are intramolecular C-HÁ Á ÁN, N-HÁ Á ÁN and C-HÁ Á ÁO hydrogen bonds, and intermolecular N-HÁ Á ÁO hydrogen bonds.

📜 SIMILAR VOLUMES

1-{[3-(4-Bromo­phen­yl)-1,2,4-oxadiazol-
1-{[3-(4-Bromo­phen­yl)-1,2,4-oxadiazol-5-yl]meth­yl}-4-[(2,6-dimethyl­phen­yl)amino­carbonyl­meth­yl]piperazine
✍ Wang, Hai-Bo ;Liu, Zhi-Qian ;Yan, Xiao-Chen 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 119 KB

The title compound, C 23 H 26 BrN 5 O 2 , was synthesized by the reaction of 4- [(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine and 3-(3-nitrophenyl)-5-chloromethyl-1,2,4-oxadiazole. There are intramolecular C-HÁ Á ÁN and intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds in the crystal struc

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✍ Yang, Shu-Ping ;Han, Li-Jun ;Wang, Da-Qi ;Ding, Tie-Zhu 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 361 KB

Molecules of the title compound, C 24 H 26 N 4 , are linked by C-HÁ Á ÁN hydrogen bonds, forming a C(5) chain along the [010] direction. Neighboring chains are connected by four C-HÁ Á Á interactions, resulting in the formation of a threedimensional network.

Meth­yl 3-(dimethyl­amino)-2-(2-{2-(dime
Meth­yl 3-(dimethyl­amino)-2-(2-{2-(dimethyl­amino)-1-[3-(2-methyl­phen­yl)-1,2,4-oxadiazol-5-yl]vinylox­y}phen­yl)acrylate
✍ Pu, Yue-Qing ;Wang, Hai-Bo ;Chen, Jia-Hui ;Wang, Jin-Tang 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 333 KB

The title compound, C 25 H 28 N 4 O 4 , was synthesized by the reaction of methyl 2-{[3-(2-methylphenyl)-1,2,4-oxadiazol-5yl]methoxy}phenyl acetate and N,N-dimethylformamide dimethyl acetal. In the crystal structure, there are intramolecular C-HÁ Á ÁO and C-HÁ Á ÁN hydrogen bonds and intermolecular

5-Chloro­meth­yl-3-(3-methoxy­phen­yl)-1
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✍ Wang, Hai-Bo ;Pu, Yue-Qing ;Chen, Jia-Hui ;Wang, Jin-Tang 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 235 KB

In the structure of the title compound, C 10 H 9 ClN 2 O 2 , there is a weak intramolecular C-HÁ Á ÁN interaction, and intermolecular C-HÁ Á ÁO and C-HÁ Á ÁN interactions.

1-{(2-Chloro­phen­yl)[(4-methyl­phen­yl)
1-{(2-Chloro­phen­yl)[(4-methyl­phen­yl)imino]meth­yl}ferrocene
✍ Wang, Hong-Xing ;Zhou, Hui-Chao ;Wu, Hong-Fei 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 127 KB

The title compound, [Fe(C 5 H 5 )(C 19 H 15 ClN)], a new ketiminecontaining ferrocenyl derivative, has been synthesized and characterized structurally. Conjugation between the two benzene rings and the imine group is not observed. In addition, there are no significant intermolecular interactions.