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Isomerisation and conformation studies of (+)- and (−)6-hydroxy-5, 6-dihydrouridine

✍ Scribed by R. Ducolomb; J. Cadet; C. Taïeb; R. Teoule

Book ID
115746208
Publisher
Elsevier Science
Year
1976
Weight
499 KB
Volume
432
Category
Article
ISSN
0005-2787

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✍ Vinko Škarić; Jasenka Matulić-Adamić 📂 Article 📅 1983 🏛 John Wiley and Sons 🌐 German ⚖ 453 KB

## Abstract The hydrogenation of 2′, 3′‐__O__‐isopropylidene‐5‐methyluridine **(1)** in water over 5% Rh/Al~2~O~3~ gave (5 __R__)‐ and (5 __S__)‐5‐methyl‐5, 6‐dihydrouridine **(2)**, separated as 5′‐__O__‐(__p__‐tolylsulfonyl)‐ **(3)** and 5′‐__O__‐benzoyl‐ **(5)** derivatives by preparative TLC. o