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Isocyanates derived from fatty acids by the trimethylsilyl azide modification of the curtius rearrangement

✍ Scribed by S. S. Washburne; W. R. Peterson

Book ID
112795835
Publisher
Springer-Verlag
Year
1972
Tongue
English
Weight
225 KB
Volume
49
Category
Article
ISSN
0003-021X

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πŸ“œ SIMILAR VOLUMES

A facile synthesis of primary amines fro
A facile synthesis of primary amines from carboxylic acids by the curtius rearrangement
✍ Todd L. Capson; C.Dale Poulter πŸ“‚ Article πŸ“… 1984 πŸ› Elsevier Science 🌐 French βš– 197 KB

Ab4tic.Z . 2-Trimethylsilylethanol was used to trap isocyanates produced by the Curtius rearrangement of acyl azides and the resulting trimethylsilylethyl carbamates were readily cleaved with tetra-n-butylammonium fluoride to liberate the primary amines.