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Hydrothermal synthesis, structural approach, magnetic and Mössbauer study of the layered Fe(III) carboxyethylphosphonate [Fe(OH)(H2O)(O3P-(CH2)2-CO2H)] or MIL-37

✍ Scribed by Myriam Riou-Cavellec; Morgane Sanselme; Jean-Marc Grenèche; Gérard Férey


Book ID
114370250
Publisher
Elsevier Science
Year
2000
Tongue
English
Weight
464 KB
Volume
2
Category
Article
ISSN
1293-2558

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📜 SIMILAR VOLUMES


Hydrothermal Synthesis, Structure, and M
✍ Morgane Sanselme; Myriam Riou-Cavellec; Jean-Marc Grenèche; Gérard Férey 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 412 KB

Fe III (H 2 O)(O 3 P-(CH 2 )-CO 2 )] or MIL-49 was hydrothermally synthesized under autogenous pressure at 1701C for 48 h. Its bidimensional structure was solved from single-crystal X-ray diffraction in the monoclinic space group P2 1 /c (No.14). Cell parameters are a = 9.3836(3) A ˚, b = 6.3798(3)

Hydrothermal Synthesis, Powder Structura
✍ M. Riou-Cavellec; C. Serre; J. Robino; M. Noguès; J.-M. Grenèche; G. Férey 📂 Article 📅 1999 🏛 Elsevier Science 🌐 English ⚖ 651 KB

Fe 2 (H 2 O) 2 (O 3 P+CH 2 +PO 3 H) 2 ](H 2 O) 2 or MIL-13 was prepared hydrothermally (120 h at 473 K). Its structure was determined by powder X-ray di4raction. This compound crystallizes in the triclinic system (P-1) with the following cell parameters: a ‫؍‬ 9.8487(6) A > , b ‫؍‬ 8.0308(5) A > , c

Synthesis, Crystal Structure, and IR and
✍ G. Giester; A. Beran; G.J. Redhammer 📂 Article 📅 1997 🏛 Elsevier Science 🌐 English ⚖ 770 KB

The representatives of the new isotypic series M 3 Fe 2 (SeO 3 ) 6 • 2H 2 O (M ‫؍‬ Mg, Co, Ni) were prepared at 500 K from aqueous solutions, kept in Teflon-coated autoclaves. Their crystal structures were determined by direct methods from single-crystal X-ray diffraction data in the space group P1