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Synthesis, structure of [H3dien]·(MF6)·H2O (M=Cr, Fe) and 57Fe Mössbauer study of [H3dien]·(FeF6)·H2O

✍ Scribed by Amor Ben Ali; Minh Trang Dang; Jean-Marc Grenèche; Annie Hémon-Ribaud; Marc Leblanc; Vincent Maisonneuve

Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
593 KB
Volume
180
Category
Article
ISSN
0022-4596

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✍ L. Asch; I. Dézsi; T. Lohner; B. Molnár 📂 Article 📅 1976 🏛 Elsevier Science 🌐 English ⚖ 205 KB

The Miissbauer spectra of iron and cobalt fluoroborate hexahydrate show a change by a factor of two in the quadrupole interaction near 2%) K and 185 K, respectively, togtther with a sudden drop in resonance fraction. This behaviour is explained as a first order phase transition in which the axial pa