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Synthesis, structure and metamagnetic behaviour of a three-dimensional Fe(II) carboxyethylphosphonate: [Fe3(OH)2(H2O)4(O3P(CH2)2CO2H)2] or MIL-38

✍ Scribed by Myriam Riou-Cavellec; Morgane Sanselme; Marc Noguès; Jean-Marc Grenèche; Gérard Férey

Book ID
114370577
Publisher
Elsevier Science
Year
2002
Tongue
English
Weight
259 KB
Volume
4
Category
Article
ISSN
1293-2558

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📜 SIMILAR VOLUMES

Hydrothermal Synthesis, Structure, and M
Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Fe(III) Carboxymethylphosphonate: [Fe(H2O)(O3P–CH2–CO2)] or MIL-49
✍ Morgane Sanselme; Myriam Riou-Cavellec; Jean-Marc Grenèche; Gérard Férey 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 412 KB

Fe III (H 2 O)(O 3 P-(CH 2 )-CO 2 )] or MIL-49 was hydrothermally synthesized under autogenous pressure at 1701C for 48 h. Its bidimensional structure was solved from single-crystal X-ray diffraction in the monoclinic space group P2 1 /c (No.14). Cell parameters are a = 9.3836(3) A ˚, b = 6.3798(3)

Hydrothermal Synthesis, Powder Structura
Hydrothermal Synthesis, Powder Structural Determination, and Magnetic Study of the Novel Hydrated Iron Diphosphonate [Fe2(H2O)2(O3P–CH2–PO3H)2](H2O)2 or MIL-13
✍ M. Riou-Cavellec; C. Serre; J. Robino; M. Noguès; J.-M. Grenèche; G. Férey 📂 Article 📅 1999 🏛 Elsevier Science 🌐 English ⚖ 651 KB

Fe 2 (H 2 O) 2 (O 3 P+CH 2 +PO 3 H) 2 ](H 2 O) 2 or MIL-13 was prepared hydrothermally (120 h at 473 K). Its structure was determined by powder X-ray di4raction. This compound crystallizes in the triclinic system (P-1) with the following cell parameters: a ‫؍‬ 9.8487(6) A > , b ‫؍‬ 8.0308(5) A > , c