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Hydrazine determination in sludge samples by high-performance liquid chromatography

✍ Scribed by Gracy Elias; William F. Bauer

Publisher: John Wiley and Sons
Year: 2006
Tongue: English
Weight: 499 KB
Volume: 29
Category: Article
ISSN: 1615-9306
DOI: 10.1002/jssc.200500380

No coin nor oath required. For personal study only.

✦ Synopsis

Hydrazine determination in sludge samples by high-performance liquid chromatography

A relatively simple and cost-effective method utilizing HPLC with UV detection was developed to detect and quantify hydrazine in sludge samples. The method was developed primarily for sludge samples, but it can also be applicable to soil and other environmental samples. The hydrazines in the matrices were derivatized to hydrazones with benzaldehyde. The hydrazones were separated using HPLC with an RP C-18 column in an isocratic mode with methanol-water (95:5 v/v) and detected with UV detection at 313 nm. The detection limit (25 lL injection) for the method is 0.02 lg/mL of hydrazine.

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