Proton decoupling is a crucial step to obtain high-resolution NMR spectra of macromolecules. Current methods employ phase (or amplitude)-modulated radio-frequency pulses to this end. To be effective, the modulation has to match some resonant condition. We demonstrate in this Communication a simple a
Heteronuclear Recoupling in Solid-State Magic-Angle-Spinning NMR via Overtone Irradiation
โ Scribed by Wi, Sungsool; Frydman, Lucio
- Book ID
- 127075138
- Publisher
- American Chemical Society
- Year
- 2001
- Tongue
- English
- Weight
- 140 KB
- Volume
- 123
- Category
- Article
- ISSN
- 0002-7863
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