𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Resolution of Sample Heterogeneity in Solid-State NMR Dipolar Recoupling and Magic Angle Spinning Sideband Analyses

✍ Scribed by Gehman, John D.; Sani, Marc-Antoine; Mehta, Anil K.


Book ID
122169567
Publisher
Biophysical Society
Year
2011
Tongue
English
Weight
36 KB
Volume
100
Category
Article
ISSN
0006-3495

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


Increasing the robustness of heteronucle
✍ Guillaume Gerbaud; Fabio Ziarelli; Stefano Caldarelli πŸ“‚ Article πŸ“… 2003 πŸ› Elsevier Science 🌐 English βš– 282 KB

Proton decoupling is a crucial step to obtain high-resolution NMR spectra of macromolecules. Current methods employ phase (or amplitude)-modulated radio-frequency pulses to this end. To be effective, the modulation has to match some resonant condition. We demonstrate in this Communication a simple a

Advanced solid-state NMR spectroscopy of
✍ Hafner, S. ;Spiess, H. W. πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 English βš– 515 KB

Continuing recent progress in the design of magic angle spinning MAS equipment now allows spinning frequencies of up to 35 kHz in commercial MAS probes. Such high frequencies make MAS an important tool for the manipulation of strong dipolar couplings, in particular when supplemented by suitable puls

High-resolution solid state 13C NMR stud
✍ Ian J. Shannon; Kenneth D.M. Harris; S. Arumugam πŸ“‚ Article πŸ“… 1992 πŸ› Elsevier Science 🌐 English βš– 621 KB

High-resolution solid state "C NMR spectra of polycrystalline ferrocene have been recorded, at room temperature, under conditions of magic angle sample spinning and high power 'H decoupling. It is shown that, contrary to naive expectations, the linewidth of the isotropic peak in the spectrum increas

Rotor Modulations and Recoupling Strateg
✍ Ingrid Fischbach; Florian Ebert; Hans Wolfgang Spiess; Ingo Schnell πŸ“‚ Article πŸ“… 2004 πŸ› John Wiley and Sons 🌐 English βš– 397 KB

## Abstract Recoupling strategies for anisotropic interactions enable the investigation of molecular structure, order and dynamics in a sensitive and site‐specific fashion by solid‐state NMR spectroscopy. Whereas magic‐angle spinning (MAS) efficiently averages anisotropic interactions and enhances