A method is described for the synthesis of a [13C]c~-mannosyl glycolipid analog from [13C]glucose. After acetylation and reduction of glucose (U-13C6, 30%) to tri-O-acetyl-D-glucal (U-13C6, 30%), addition of the nucleophile 2-[2-[2-[2-(tetradecyloxy)ethoxy]ethoxy]ethoxy]-ethanol (tetra-decyltetragly
Gram-scale synthesis and efficient purification of 13 C-labeled levoglucosan from 13 C glucose
✍ Scribed by Alexander, Lisa; Hoyt, Caroline; Michalczyk, Ryszard; Wu, Ruilian; Thorn, Dave L.; Silks, L. A. ‘Pete’
- Book ID
- 118762945
- Publisher
- John Wiley and Sons
- Year
- 2012
- Tongue
- French
- Weight
- 126 KB
- Volume
- 56
- Category
- Article
- ISSN
- 0022-2135
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