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Formation of Edge-Sharing BO4 Tetrahedra in the High-Pressure Borate HP-NiB2O4

✍ Scribed by Johanna S. Knyrim; Felix Roeßner; Stefanie Jakob; Dirk Johrendt; Isabel Kinski; Robert Glaum; Hubert Huppertz

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
507 KB
Volume
46
Category
Article
ISSN
0044-8249

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✍ Stephanie C. Neumair; Reinhard Kaindl; Hubert Huppertz 📂 Article 📅 2012 🏛 John Wiley and Sons ⚖ 21 KB 👁 1 views

Hydrate Borate. -Violet, air-and water-resistant crystals of the title compound are synthesized from a stoichiometric mixture of Co3O4 and H3BO3 (Walker-type multianvil apparatus, 6 GPa, 880 °C, 5 min). The new high--pressure phase is characterized by powder and single crystal XRD, IR, and Raman spe