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High-Pressure Synthesis of α-Ln2B4O9 (Ln: Sm, Ho), with a Structure Type Displaying Edge-Sharing BO4 Tetrahedra.

✍ Scribed by Holger Emme; Hubert Huppertz

Publisher: John Wiley and Sons
Year: 2005
Weight: 14 KB
Volume: 36
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200523010

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## Abstract High‐pressure/high‐temperature conditions of 10 GPa and 1150 °C were used to synthesize the new rare‐earth oxoborates __α__‐(RE)~2~B~4~O~9~ (RE=Eu, Gd, Tb, Dy) in a Walker‐type multianvil apparatus. Single‐crystal X‐ray structure determination of __α__‐(RE)~2~B~4~O~9~ (RE=Eu, Gd, Tb) re