Entrapped copper(II) carbonate for indirect determination of glycine by flow injection atomic absorption spectrometry
✍ Scribed by J.V. Garcia Mateo; J.Martínez Calatayud
- Publisher
- Elsevier Science
- Year
- 1993
- Tongue
- English
- Weight
- 556 KB
- Volume
- 274
- Category
- Article
- ISSN
- 0003-2670
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✦ Synopsis
Copper(H) carbonate was physically entrapped m a polyester during polymenzatlon The resulting solid resin was used as a reactor for glycme determmatlon by means of a flow mlectlon mamfold and applied to pharmaceutical formulations, the glycme complexed wth and thus dissolved some of the munobdlzed C&I), which was monitored by an atonuc absorption spectrometer The calibration graph IS hnear m the range 12-35 kg ml-' glycme, the detectlon limit IS 12 pg ml-', the relative standard deviation at 20 pg ml-' IS 1 1% (n = 20) and the sample throughput IS 180 h-'
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Ahstraet A method for entrapment of reagents IS described The expcnmental procedure IS based on the dlsperslon of the reagent (MnOz) mto an unsaturated polyester solution and gnndmg the product to give the required particle size (300-400 pm) The reagent 1s packed mto a bed reactor (15 mm I d I and i