The enantiomeric characterization of methamphetamine is readily accomplished by 'H-NMR analysis of the diastereomers formed by derivatization with 2,3,4,6-tetra-O-acetylcetyl-8-D glucopyranosyl isothiocyanate (GITC). The stereospecific chemical shifts of a host of signals from the GITC moiely provid
Determination of the Synthetic Origin of Methamphetamine Samples by 2 H NMR Spectroscopy
โ Scribed by Armellin, Silvia; Brenna, Elisabetta; Frigoli, Samuele; Fronza, Giovanni; Fuganti, Claudio; Mussida, Daniele
- Book ID
- 118070263
- Publisher
- American Chemical Society
- Year
- 2006
- Tongue
- English
- Weight
- 218 KB
- Volume
- 78
- Category
- Article
- ISSN
- 0003-2700
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
## Abstract The paper briefly reviews the process of determining the structures of membrane proteins by NMR spectroscopy of aligned samples, describes the integration of recent developments in the interpretation of spectra of aligned proteins and illustrates the application of these methods to the
We demonstrate the application of the proton inverse detected deuteron (PRIDE) NMR technique to the measurement of the orientation of membrane-bound peptides with enhanced sensitivity. Gramicidin D, a transmembrane peptide, and ovispirin, a surfacebound peptide, were used as model systems. The pepti