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Detection of 2-Amino-1-methyl-6-(4-hydroxyphenyl)imidazo[4,5-b]pyridine in Broiled Beef

✍ Scribed by Kurosaka, Reiko ;Wakabayashi, Keiji ;Ushiyama, Hirofumi ;Nukaya, Haruo ;Arakawa, Nobuhiko ;Sugimura, Takashi ;Nagao, Minako

Book ID: 108579518
Publisher: Wiley (Blackwell Publishing)
Year: 1992
Tongue: English
Weight: 236 KB
Volume: 83
Category: Article
ISSN: 0910-5050
DOI: 10.1111/j.1349-7006.1992.tb02000.x

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## Abstract The syntheses of the deuterium‐labeled food mutagen 2‐amino‐1‐methyl‐6‐phenyl‐1H‐imidazo[4,5‐b]pyridine (PhIP) and its __N__‐hydroxy metabolite are described. Unlabeled PhIP is deuterated using a boron trifluoride phosphoric acid complex in one step. Labeled PhIP–^2^H~5~ is nitrosated t