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Crystal Structure of 4-Tert-Butylimino-3, 3-Diethoxycarbonyl-1-Methyl-2-Tosylimino-Azetidine

✍ Scribed by Luc Van Meervelt; Gerrit L'Abbé; Geoffrey S. D. King

Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
203 KB
Volume
95
Category
Article
ISSN
0037-9646

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✦ Synopsis

The crystal structure of 4-tert-butylimino-3,3-diethoxycarbonyl- I-methyl-2-tosylimino-azecidine ( C H N 0 S, a = 2 5 . 3 3 4 ( 4 ) , b = 8.223(1), c = 11.574(2) 1, f? = 91.88(1)', space group PZ1/n, Z = 4) has been determined by single-crystal X-Ray diffraction techniques and refined to R = 0.095 (The high R-value is ascribed to the small crystal size and also to partial disorder in a side-chain). C-C bond of 1.60(2) A. The bond lengths of the exocyclic imino functions differ significantly.

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