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Convenient Large-Scale Synthesis of d -Glucaro-1,4:6,3-dilactone

โœ Scribed by Gehret, Troy C.; Frobese, A. Stephen; Zerbe, James S.; Chenault, H. Keith

Book ID
127215898
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
736 KB
Volume
74
Category
Article
ISSN
0022-3263

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A Convenient Large-Scale Synthesis of Ethyl (2-Cyanoimino-5,6dichloro-1,2,3,4-tetrahydroquinazoline-3-yl)acetate. -A practical industrial scale synthesis of the title compound (III), a key intermediate in the synthesis of the drug anagrelide, starting from glycinate (I) is accomplished.